반응 최적화
다양한 조건에서 얻은 MRI 스펙트럼을 비교함으로써 온도, 용매, 농도와 같은 반응 조건을 최적화하기 위해 MRI 데이터를 사용할 수 있습니다.
화학 원료를 구입해야하는 경우 요청 정보를 제출하여최신견적을받으십시오.
반응 최적화의 학술 논문
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NMR studies on [2+3] cycloaddition of nitrile oxides to cyclohexene derivatives
화학 물질
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methyl (2E)-3-[(4S)-4-(2-methoxypropan-2-yl)cyclohex-1-en-1-yl]prop-2-enoate
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Synthesis of new class of spirocarbocycle derivatives by multicomponent domino reaction and their evaluation for antimicrobial, anticancer activity and molecular docking studies
화학 물질
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2-(4-methoxybenzylidene)cyclohexane-1,3-dione
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Ferrocene analogues of hydrogen-bond-donor catalysts: An investigative study on asymmetric Michael addition of 1,3-dicarbonyl compounds to nitroalkenes
화학 물질
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(S)-3-[1-(3-chlorophenyl)-2-nitroethyl]-pentane-2, 4-dione
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Buchwald-Hartwig reactions in water using surfactants
화학 물질
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카르바닐산, m-메틸-, 벤질 에스테르(6CI)
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Total Synthesis of Halicholactone and Neohalicholactone
화학 물질
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2(3H)-Furanone, dihydro-4-[(4-methoxyphenyl)methoxy]-, (4S)-
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Total Synthesis of (+)-Rubellin C
화학 물질
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4-methoxy-3-phenylthioisobenzofuran-1(3H)-one
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Thermally accelerated asymmetric hydrosilylations using ligated copper hydride
화학 물질
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(S)-ethyl 3-methyl-5-phenylpentanoate
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Biocatalytic Strategy for Highly Diastereo- and Enantioselective Synthesis of 2,3-Dihydrobenzofuran-Based Tricyclic Scaffolds
화학 물질
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7-Bromo-5-fluorobenzo[b]furan
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Electroreductive synthesis of acylsilanes from acylimidazoles
화학 물질
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Adipinsaeuremonomethylester-imidazolid
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Enantioselective metallo-organocatalyzed preparation of cyclopentanes bearing an all-carbon quaternary stereocenter
화학 물질
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dimethyl (S)-3-formyl-4-methylene-3-phenylcyclopentane-1,1-dicarboxylate
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Efficient assembly of allenes, 1,3-dienes, and 4H-pyrans by catalytic regioselective nucleophilic addition to electron-deficient 1,3-conjugated enynes
화학 물질
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trimethyl 5-(naphthalen-1-yl)-2-phenylpenta-3,4-diene-1,1,3-tricarboxylate
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Catalytic asymmetric synthesis of glutamate analogues
화학 물질
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4-((S)-2-Allylamino-2-cyano-ethyl)-5-[(S)-2-(tert-butyl-diphenyl-silanyloxy)-2-phenyl-ethyl]-isoxazole-3-carboxylic acid ethyl ester
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Total syntheses of the phytotoxic lactones herbarumin I and II and a synthesis-based solution of the pinolidoxin puzzle
화학 물질
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1,6-DI-O-아세틸-2,3-이소프로필리덴-D-리보스
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Total synthesis of (+)-trans-195A
화학 물질
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(2S,6R)-N-(2-nitrobenzenesulfonyl)-6-pent-4-enyl-2-propyl-1,2,3,6-tetrahydropyridine
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A FORMAL STEREOCONTROLLED SYNTHESIS OF (+/-) ISOCLOVENE
화학 물질
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Toluene-4-sulfonic acid (1S,6S,7R)-1-methyl-5-oxo-bicyclo[4.3.1]dec-7-yl ester
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Intramolecular [2+2] photocycloaddition of N-alkenoyl β - enaminones
화학 물질
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N-benzyl-N-(3-oxocyclohex-1-enyl)pent-4-enamide
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A highly convergent total synthesis of the spiroacetal macrolide (+)-milbemycin β1
화학 물질
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(+)-R-5-(tert-butyldiphenylsilyloxy)-4-methyl-1-pentyne
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Optimized Monofluoromethylsulfonium Reagents for Fluoromethylene-Transfer Chemistry
화학 물질
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(fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate
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2
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NaH
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STEREOCONTROLLED TOTAL SYNTHESIS OF THE MACROCYCLIC LACTONE (-)-ASPICILIN
화학 물질
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2H-Pyran, tetrahydro-2-[[10-(phenylmethoxy)-7-undecynyl]oxy]-, (10R)-
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Preparation of eight-membered cyclic ethers by Lewis acid promoted acetal-alkene cyclizations
화학 물질
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2-(2-phenylethyl)-3,6,7,8-tetrahydro-2H-oxocin
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<1,2-Benzenediolato(2-)-O-O'>oxotitanium. A Chemoselective and Efficient Catalyst for Aldol-type Reaction of Ketene Silyl Acetals with Aldehydes
화학 물질
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2,2-Dimethyl-3-phenyl-3-trimethylsilanyloxy-propionic acid isobutyl ester
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Total synthesis of (-)-aplaminal
화학 물질
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(-)-aplaminal
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Scaling-out pharmaceutical reactions in an automated stop-flow microwave reactor
화학 물질
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S-(4-nitrophenyl) dimethylcarbamothioate
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Total synthesis of (-)-tamandarin B
화학 물질
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4-amino-5-methyl-3-triisopropylsilanyloxy-hexanoic acid 1-[1-(2-{[1-(2-tert-butoxycarbonylamino-2-carboxy-1-methyl-ethoxycarbonyl)-2-(4-methoxy-phenyl)-ethyl]-methyl-carbamoyl}-pyrrolidine-1-carbonyl)-3-methyl-butylcarbamoyl]-2-methyl-propyl ester
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Highly diastereodivergent synthesis of tetrasubstituted cyclohexanes catalyzed by modularly designed organocatalysts
화학 물질
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(1R,2S,3R,4S)-3-nitro-4-(2-oxo-2-phenylethyl)-2-phenylcyclohexanecarbaldehyde
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Direct synthesis of substituted pyrimidines and quinazolines
화학 물질
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C19H20N2O2
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Intermolecular C-H amination of complex molecules: Insights into the factors governing the selectivity
화학 물질
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(1S,6R)-N-[N-(S)-(p-toluenesulfonyl)-p-toluenesulfonimidoyl]-3-methyl-6-(prop-1-en-2-yl)cyclohex-2-enamine
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Insight into the mechanism of the asymmetric ring-opening aminolysis of 4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]octane catalyzed by titanium/BINOLate/ water system: Evidence for the Ti(BINOLate)2-bearing active catalyst entities and the role of water
화학 물질
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(5S,6R)-6-(N-benzylacetamido)-2,2-dimethyl-1,3-dioxepan-5-yl acetate.
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Carbodiimide mediated synthesis of 4-thiazolidinones by one-pot three-component condensation
화학 물질
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4-Thiazolidinone, 2-(4-chlorophenyl)-3-cyclohexyl-
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Highly regioselective asymmetric copper-catalyzed allylic alkylation with dialkylzincs using monodentate chiral spiro phosphoramidite and phosphite ligands
화학 물질
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(11AR)-(+)-10,11,12,13-TETRAHYDRODIINDENO[7,1-DE:1',7'-FG][1,3,2]DIOXAPHOSPHOCIN-5-PHENOXY
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A new methodology for synthesis of a chiral phosphinocarboxylic acid through michael cyclization-aldol tandem reaction of chiral α,β,χ,ψ-unsaturated bisphosphine oxide and application in palladium-catalyzed asymmetric allylic alkylation
화학 물질
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2-(diphenylphosphonoyl)-2-[(1S,2S,3S,5S)-5-(diphenylphosphonoyl)-2,3-dimethoxycyclopentyl]-1-phenylethanol
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Metalation reactions XIII. The reactions of electrophiles with the dilithiated species 1-(α-lithiomethyl)-2-<(α-lithiomethyl)thio>benzene
화학 물질
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1-Ethyl-2-(ethylthio)benzene
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Regioselective ring opening of oxiranes catalysed by montmorillonite clay: A simple synthesis of β-hydroxy sulfones
화학 물질
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6-(Toluene-4-sulfonyl)-decan-5-ol
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Microwave-assisted rhodium-complex-catalyzed cascade decarbonylation and asymmetric Pauson-Khand-type cyclizations
화학 물질
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3a,4-dihydro-6-(4-methylphenyl)-1H-cyclopenta[c]furan-5(3H)-one
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Total Synthesis of Termicalcicolanone A via Organocatalysis and Regioselective Claisen Rearrangement
화학 물질
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5'-hydroxy-4-nitro-2,2',5-trifluorobenzophenone
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Reaction of Acyl Chlorides with in Situ Formed Zinc Selenolates: Synthesis of Selenoesters versus Ring-Opening Reaction of Tetrahydrofuran
화학 물질
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Se-phenyl 2-bromobenzeneselenoate
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Co(II)-Catalyzed Regioselective Cross-Dehydrogenative Coupling of Aryl C-H Bonds with Carboxylic Acids
화학 물질
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pyridine-2-carboxylic acid benzhydryl-amide
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Sequential Photoredox Catalysis for Cascade Aerobic Decarboxylative Povarov and Oxidative Dehydrogenation Reactions of N-Aryl α-Amino Acids
화학 물질
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(2-ethyl-6-methoxy-3-methyl-1,2,3,4-tetrahydro-quinolin-4-yl)-(4-methoxy-phenyl)-amine
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An efficient base-mediated intramolecular condensation of 2-(disubstituted amino)-benzonitriles to 3-aminoindoles
화학 물질
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2-phenyl-1-propyl-1H-indol-3-amine
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A facile synthesis of (+)-L-discadenine and its deuterio derivatives
화학 물질
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C14H18(2)H2N6O2
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